This shows you the differences between two versions of the page.
| Both sides previous revision Previous revision Next revision | Previous revision | ||
|
recrystallization:equipment [2011/07/09 07:54] jj |
recrystallization:equipment [2011/07/15 04:59] (current) 91.66.178.175 |
||
|---|---|---|---|
| Line 4: | Line 4: | ||
| - | 1 L hydrochloric (35-8%) = Salzsäure (33% seems easy to get) ORDERED | + | 1 L hydrochloric (35-8%) = Salzsäure (33% seems easy to get) - arrived |
| - | 1 L nitric (70% +) = salpetersäure (65%?) - http:// | + | 1 L nitric (70% +) = salpetersäure (65%?) - http:// |
| - | 2 L sulphuric (drain cleaner often around 90%, tho' chemistry uncoloured @ 95+% better) = schwefelsäure | + | 2 L sulphuric (drain cleaner often around 90%, tho' chemistry uncoloured @ 95+% better) = schwefelsäure |
| - | baking soda (Sodium bicarbonate) | + | baking soda (Sodium bicarbonate) |
| - | distilled water (2 L +) | + | small amount of Corn Syrup - supermarket |
| - | small bottle methylated spirits | + | table salt - supermarket |
| + | |||
| + | distilled water (2 L +) - chemist | ||
| glass electroytic baths/bowls | glass electroytic baths/bowls | ||
| + | battery charger [M] | ||
| - | battery charger | + | hotplate [M to get from cellar] |
| - | hotplate | + | MAPP gas - hellweg |
| - | MAPP gas | + | welding gloves - hellweg |
| - | welding gloves | ||
| - | googles | + | goggles - hellweg |
| - | pincers/ | ||
| - | coffee filters | + | pincers/ |
| - | water spray bottle(s) | + | tin snips - hellweg |
| + | |||
| + | sandpaper/ | ||
| + | |||
| + | |||
| + | coffee filters - supermarket | ||
| + | |||
| + | water spray bottle(s) - hellweg | ||
| + | |||
| + | heat gun, soldering irons/ | ||
| + | |||
| + | computer PSU, wire, small electronics kit, cables, | ||
| + | |||
| + | gherkin/etc glass jars [M] | ||
| Line 40: | Line 54: | ||
| **'' | **'' | ||
| - | heat resistant glassware - 6 x 250; 3 x 600ml beakers | + | heat resistant glassware - 6 x 250; 3 x 600ml beakers |
| + | |||
| + | vapour masks (x 3) **X** | ||
| + | |||
| + | goggles (x 8) **X** | ||
| + | |||
| + | butyl gloves/ nitrile gloves **X** | ||
| - | vapour masks (x 3) | + | gas burner head **X** |
| - | goggles (x 4-6) | + | ceramic blanket **X** |
| - | butyl gloves/ nitrile gloves | + | alumina boat(s) **X** |
| - | gas burner head | + | lead **X** |
| - | ceramic blanket | + | copper **X** |
| - | alumina boat(s) | + | chemistry filters **X** |
| - | lead | + | st.steel gauzes **X** |
| - | copper | + | syringes **X** |
| - | chemistry filters | + | sodium citrate **X** |
| - | st.steel gauzes (?) | + | micro scales **X** |
| - | syringes | + | funnels (x3) **X** |
| + | pliers, pincers (6 or so) **X** | ||
| + | webcam **X** | ||